The X-Ray Crystal Structure Analysis and Chemical Syntheses of Some Amino-Phosphine Complexes

Mokuolu, Joseph Ayinla Adebayo (1965) The X-Ray Crystal Structure Analysis and Chemical Syntheses of Some Amino-Phosphine Complexes. PhD thesis, University of Glasgow.

Abstract

The work described in this thesis is divided into five main parts and one appendix. Parts I-III deal with the accounts of the X-Ray studies of three derivatives of bis-(diphenyl-phoaphino)-ethylemine, (C6H5)2P.N.(C2H5)P(C6H5)2. Part IV describes the crystal structure analysis of lead thiocyanate and Part V summarises the chemical syntheses of some aminophosphine complexes. The appendix contains some of the methods and theories used in X-Ray Crystallography. In all the X-Ray work, the heavy atom technique was used to overcome the phase problem. Intensities ware estimated visually and the refinement of each structure was by the three-dimensional least-squares analysis.

• Item Type: Thesis (PhD)
• Qualification Level: Doctoral
• Keywords: Physical chemistry, Inorganic chemistry
• Date of Award: 1965
• Depositing User: Enlighten Team
• Unique ID: glathesis:1965-77146
• Copyright: Copyright of this thesis is held by the author.
• Date Deposited: 14 Jan 2020 09:18
• Last Modified: 14 Jan 2020 09:18
• URI: https://theses.gla.ac.uk/id/eprint/77146